物理化学学报 >> 2005, Vol. 21 >> Issue (04): 443-445.doi: 10.3866/PKU.WHXB20050420

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制备不同孔径的氧化铝模板

韩凤梅; 郭燕川; 彭必先; 陈丽娟   

  1. 中国科学院理化技术研究所，北京100101
  • 收稿日期:2004-08-01 修回日期:2004-11-11 发布日期:2005-04-15
  • 通讯作者: 陈丽娟 E-mail:chenlj@ipc.ac.cn

Preparation of Alumina Template with Different Pore Diameters

HAN Feng-Mei; GUO Yan-Chuan; PENG Bi-Xian; CHEN Li-Juan   

  1. Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100101
  • Received:2004-08-01 Revised:2004-11-11 Published:2005-04-15
  • Contact: CHEN Li-Juan E-mail:chenlj@ipc.ac.cn

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摘要： 将适量的有机溶剂加入电解液中，在15 ℃左右制备得到孔径大于200 nm的氧化铝模板.该法使电解时间缩短，加快了制备模板的过程， 是氧化铝模板的有效制备方法.将该方法与传统方法相结合，可以制备孔径在20～250 nm间的氧化铝模板. 实验表明：有机溶剂的加入可有效避免电解时热量的迅速产生, 通过改变实验条件可调控氧化铝模板的孔径.

关键词: 氧化铝模板, 有机溶剂, 孔径

Abstract: Alumina templates with large-size pores ( > 200 nm) were fabricated by adding organic solvent to electrolyte at 15 ℃. This effective method can shorten electrolysis time and quicken the process of the template preparation. A series of templates with different diameters (20～250 nm) were obtained by the combination of this method and traditional one. Experiment results show that the addition of organic solvent can efficiently avoid the heat produced quickly in the process of electrolysis. Pore diameter of alumina templates relys on controlled the experiment condition.

Key words: Alumina template, Organic solvent, Pore diameter