Acta Phys. -Chim. Sin. ›› 2026, Vol. 42 ›› Issue (2): 100164.doi: 10.1016/j.actphy.2025.100164
• REVIEW • Previous Articles Next Articles
Engineering efficient metal-organic frameworks for photocatalytic CO2 reduction
Guoqiang Peng1, Xiuyan Li2, Min Li1, Zhibo Su1, Falu Hu1,*(
), Guowei Zhou1,*()
- 1 Key Laboratory of Fine Chemicals in Universities of Shandong, Jinan Engineering Laboratory for Multi-scale Functional Materials, School of Chemistry and Chemical Engineering, Qilu University of Technology (Shandong Academy of Sciences), Jinan 250353, Shandong Province, China
2 School of Chemical Engineering and Environment, Shandong Engineering Research Center of Green and High-Value Marine Fine Chemical, Weifang University of Science and Technology, Weifang 262700, Shandong Province, China
-
Received:2025-07-12Revised:2025-08-14Accepted:2025-08-17Published:2025-12-03 -
Contact:Email: faluhu@qlu.edu.cn (Falu Hu)gwzhou@qlu.edu.cn (Guowei Zhou)
Cite this article
Guoqiang Peng, Xiuyan Li, Min Li, Zhibo Su, Falu Hu, Guowei Zhou. Engineering efficient metal-organic frameworks for photocatalytic CO2 reduction[J]. Acta Phys. -Chim. Sin. 2026, 42(2), 100164. doi: 10.1016/j.actphy.2025.100164
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Fig 1
(a) Synthesis of UiO-68-X (X= –F, –CH3, –OCH3). (b) Photocatalytic CO evolution. Reprinted with permission from Ref. [104], Copyright 2019, Royal Society of Chemistry. (c) Synthesis of Zr-MOF-X (X = PA, SA, BA, and TA). (d) HCOOH production. Reprinted with permission from Ref. [105], Copyright 2022, Elsevier."
Fig 2
(a) Synthesis of UiO-68-Fe-bpy. (b) CO evolution of UiO-68-NH2, TPDC-Fe-bpy and UiO-68-Fe-bpy. Reprinted with permission from Ref. [106], Copyright 2020, Royal Society of Chemistry. (c) Synthesis of 66-IS-M and its photocatalytic mechanism. (d) CO and H2 produced over NH2-UiO-66, 66-IS, 66-IS-Ni, 66-IS-Co, and 66-IS-Cu. Reprinted with permission from Ref. [107], Copyright 2023, American Chemical Society."
Fig 3
(a) Structure of PCN-222. (b) The HCOO− production yields of {(a) PCN-222, (b) H2TCPP, (c) no PCN-222, (d) no TEOA, and (e) no CO2}. Reprinted with permission from Ref. [108], Copyright 2015, American Chemical Society. (c) Synthesis and structure of the In-Fe/CoTCPP-MOF. (d) The CO evolution catalyzed by In-Fe1.91TCPP-MOF, In-Co1.71TCPP-MOF, and In-InTCPP-MOF under irradiation with a 300 W xenon light (>400 nm). Reprinted with permission from Ref. [109], Copyright 2020, American Chemical Society. (e) Structure of ZrPP-1. (f) The CO production yields of ZrPP-1-M under visible-light irradiation. Reprinted with permission from Ref. [110], Copyright 2017, Wiley-VCH."
Fig 4
(a) Thermally induced 2D porphyrin MOF IHEP-21 conversion to 3D porphyrin MOF IHEP-22 and IHEP-23. Reprinted with permission from Ref. [112], Copyright 2023, American Chemical Society. (b) Crystal structures and characterization of MOFs. Macrocyclic π-electron of linkers {(A) TBCP, (B) TBML, (C) TML, (D) TM, and (E) TNP. Crystal structures of MOFs (F) TBCP-MOF, (G) TBML-MOF, (H) TML-MOF, (Ⅰ) TM-MOF, and (J) TNP-MOF}. Reprinted with permission from Ref. [113], Copyright 2022, American Chemical Society."
Fig 5
(a) Synthetic procedure of ZBU-Co. Reprinted with permission from Ref. [114], Copyright 2023, Springer Nature. (b) Synthetic scheme of Co-UiO-67 or Re-UiO-67. (c) Evolution of CO under 300 W Xe lamp irradiation for 4 h. Reprinted with permission from Ref. [115], Copyright 2020, American Chemical Society."
Fig 6
(a) The synthetic procedure of UiO-bpydc(M), M = Ce or Zn. (b) TON of CO2 cycloaddition reaction under light illumination over UiO-bpydc, UiO-bpydc(Ce) and UiO-bpydc(Zn). Reprinted with permission from Ref. [116], Copyright 2021, Elsevier. (c) Synthesis of the two-dimensional Fe/Ti-BPDC (d) Proposed photocatalytic mechanism of CO2 to HCOOH over Fe/Ti-BPDC. Reprinted with permission from Ref. [117], Copyright 2023, Elsevier."
Fig 7
(a) Synthesis of AUBM-4. (b) Proposed mechanism for CO2 photoreduction over AUBM-4 under visible light irradiation. Reprinted with permission from Ref. [118], Copyright 2019, American Chemical Society. (c) Synthesis of LTG-FeZr. Reprinted with permission from Ref. [119], Copyright 2023, American Chemical Society."
Fig 8
(a) Schematic illustration of the mixed-ligand strategy for preparing partially fluorinated MIL-101(Fe). (b) Proposed reaction pathway for the boosted photocatalytic CO2 reduction over sensitized fluorinated MIL-101(Fe). Reprinted with permission from Ref. [122], Copyright 2023, Wiley-VCH. (c) Schematic diagram of the synthesis of the high-performance photocatalysts based on a trade-off between enhancing LMCT and frustrating Lewis acid. Reprinted with permission from Ref. [123], Copyright 2022, Elsevier. (d) Schematic illustration to engraft a donor-acceptor (PBA-MV) complex into MOF-808 (Zr) pore for visible-light-driven CO2 reduction to selective CH4. Reprinted with permission from Ref. [124], Copyright 2023, Springer Nature."
Fig 9
(a) Schematic representation of developing Zr-MBA-Ru/Mn-MOF through stepwise PSM. Reprinted with permission from Ref. [126], Copyright 2023, American Chemical Society. (b) Schematic host-guest representation with photoinduced electron transfer between triethanolamine (TEOA) and CO2 reduction. Reprinted with permission from Ref. [127], Copyright 2021, American Chemical Society. (c) Representation of integrated molecular photosystems (spheres) in various assembly-controlling MOF topologies. Reprinted with permission from Ref. [128], Copyright 2021, Wiley-VCH."
Fig 10
(a) Preparation process of Co/Fe-MOX. (b)The time-yield curves of Co/Fe-MOX. Reprinted with permission from Ref. [132], Copyright 2023, Elsevier. (c) A series of NH2-MIL-125-Ni0.5–1.5%/Ti. (d) Photocatalytic performance of as-prepared samples: CO, CH4, H2 productivity of NH2-MIL-125-Ni0.5–1.5%/Ti. Reprinted with permission from Ref. [133], Copyright 2020, Elsevier. (e) Schematic illustration of synthesis of the PCN-250-Fe3 and PCN-250-Fe2M (Mn, Zn, Ni, Co). (f) PCN-250-Fe3 and PCN-250-Fe2M for CO evolution. Reprinted with permission from Ref. [134], Copyright 2020, Elsevier. (g) Schematic of the synthesis of MCOF-Ti6Cu3. (h) Proposed mechanism of CO2 reduction and H2O oxidation. Reprinted with permission from Ref. [135], Copyright 2022, Springer Nature."
Fig 11
(a) In situ formation of frustrated Lewis pairs (FLPs) via a linker-deficient UiO-66 to activate CO2 molecules. (b) Photocatalytic results of the as-prepared samples with water. Reprinted with permission from Ref. [140], Copyright 2022, American Chemical Society. (c) Schematic illustration of varied defective structures. Reprinted with permission from Ref. [142], Copyright 2021, Elsevier. (d) Photoreduction of CO2 to CO and photoelectron evolution rates for varied samples. Reprinted with permission from Ref. [143], Copyright 2021, American Chemical Society."
Fig 12
(a) Schematic illustration of the fabrication of Ni-BDC NSs. (b) The proposed reaction mechanism for CO2 photoreduction. Reprinted with permission from Ref. [145], Copyright 2021, Wiley-VCH. (c) Synthetic illustration of the Co-MNSs for visible-light-driven photocatalytic CO2 to CO conversion. (d) Comparison of CO2 photocatalytic performance over Co-MNSs. Reprinted with permission from Ref. [147], Copyright 2023, Springer Nature. (e) Schematic diagram of the synthetic routes for preparing monolayer MOF and bilayer MOF. (f) Computational free energy diagram of CO2 reduction reaction for monolayer MOF1 and bilayer MOF2. Reprinted with permission from Ref. [148], Copyright 2023, Wiley-VCH."
Fig 13
(a) Synthetic procedures for bulky Ni-MOF, Ni-MOL-010, Ni-MOL-100. (b)The photocatalytic activities of bulky Ni-MOF, Ni-MOL-010 and Ni-MOL-100. Reprinted with permission from Ref. [149], Copyright 2020, Wiley-VCH. (c) Synthetic procedures for Fe-soc-MOFs exposed with different facets. (d) The CO and H2 yields. Reprinted with permission from Ref. [150], Copyright 2023, American Chemical Society. (e) Schematic illustration of the evolution of morphology and facet over NH2-MIL-125. (f) Yields of CO and CH4 under visible light irradiation (5 h) of NM001, NMA, NMB, NMC, and NM111. Reprinted with permission from Ref. [151], Copyright 2021, American Chemical Society."
Fig 14
(a) Schematic illustration of the evolution of morphology and facet over NH2-MIL-125 {(T1) (T2) (T3) (T12) (T13) (T23)}. (b) The yield of CO and CH4 of T1, T2, T3, T12, T13 and T23. Reprinted with permission from Ref. [152], Copyright 2021, Elsevier. (c) Synthetic scheme of as-synthesized NH2-MIL-125 (Ti) with T000, T010 and T112 facets. (d) The yield of products and apparent quantum yield. Reprinted with permission from Ref. [153], Copyright 2021, Elsevier. (e) Schematic diagram of the fabricating procedure and photocatalytic application for ultrathin nanosheets NH2-MIL-125. (f) Comparison of photocatalytic reaction rates normalized by the surface area for varied catalysts. Reprinted with permission from Ref. [154], Copyright 2022, American Chemical Society."
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