物理化学学报 >> 1997, Vol. 13 >> Issue (04): 380-384.doi: 10.3866/PKU.WHXB19970419

研究简报 上一篇    

碳化硅纳米晶须的微波合成

戴长虹,刘素兰,张显鹏   

  1. 东北大学有色金属冶金系，沈阳 110006
  • 收稿日期:1996-09-28 修回日期:1996-12-23 发布日期:1997-04-15
  • 通讯作者: 戴长虹

Microwave Synthesis of SiC Nanometer Whiskers

Dai Chang-Hong,Liu Su-Lan,Zhang Xian-Peng   

  1. Department of Nonferrous Metallurgy,Northeastern University,Shenyang 110006
  • Received:1996-09-28 Revised:1996-12-23 Published:1997-04-15
  • Contact: Dai Chang-Hong

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关键词: 碳化硅, 纳米晶须, 热解炭, 微波合成

Abstract:

SiC nanometer whisker, whose diameter was about 50nm and purity was 98.54%, was synthesized by microwave heating in an atmosphere of argon. Char pyrolyzed phenolformaldehyde resin and SiO2 nanometer powder were used as starting materials. The properties of the whisker were determined by XRD and TEM. The mechanism for synthesizing SiC nanometer whisker was discussed.

Key words: SiC, Nanometer whisker, Char, Microwave synthesis