超声分散对单壁碳纳米管分离的影响

doi:10.3866/PKU.WHXB201204174

Abstract

Abstract:

Recently, gel chromatography has been demonstrated as an effective method for the separation of single-walled carbon nanotubes (SWCNTs) according to their electronic type and structure. The separation of SWCNTs was thought to result from the different affinity forces between the gel and various SWCNTs. Based on this method, we investigated the effect of ultrasonic time on the dispersion and separation of metallic and semiconducting SWCNTs. At a low ultrasonic power, with the increase of ultrasonic time, better monodispersed SWCNTs in sodium dodecylsulfate (SDS) aqueous solution were obtained. The UV-visible-near infrared (UV-Vis-NIR) absorption, Raman and photoluminescence (PL) spectroscopic characterizations confirmed that under the condition of ultrasonication (2 h), higher-purity metallic tubes and semiconducting tubes with different diameter distributions could be obtained. We believe that the control of the ultrasonication time may tune the mono-dispersity and the length of SWCNTs, which would further influence the difference in affinity forces between various SWCNTs and the gel, therefore leading to different separation results.

Key words: Single-walled carbon nanotube, Gel column chromatography, Dispersion, Metal/semiconductor separation, Ultrasonic time

TAN Fu-Rui, LI Hong-Bo, GUI Hui, ZHANG Jing, LI Ru, JIN He-Hua. Effects of Ultrasonic Dispersion on the Separation of Single-Walled Carbon Nanotubes[J]. Acta Phys. -Chim. Sin. 2012, 28(07), 1790-1796. doi: 10.3866/PKU.WHXB201204174

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Effects of Ultrasonic Dispersion on the Separation of Single-Walled Carbon Nanotubes

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