尺寸可控的单分散四氧化三铁微球的省时制备

doi:10.3866/PKU.WHXB201706093

Abstract

Abstract:

Monodisperse Fe₃O₄ microspheres with tunable diameters and high magnetic saturation were synthesized by a solvothermal reduction method. It was found that the morphology and structure of the Fe₃O₄ microspheres could be tuned by simply altering the amount of the reactants such as ferric chloride, sodium acetate, water, and the reaction time. The Fe₃O₄ microspheres obtained via this method possessed high purity, crystallinity, and a nearly spherical shape. Furthermore, they were monodispersed and no aggregation was found. Such monodisperse Fe₃O₄ microspheres had tunable diameters of 400-700 nm and the fabrication time was only 2-4 h. The products showed high magnetic saturation values, and their yields were typically more than 94%.

Key words: Monodisperse Fe₃O₄ microspheres, Solvothermal, Time-saving, Tunable

Dan WANG,Chuan-Yong LIU,Yue LONG,Kai SONG,Wei HUANG. A Time-Saving Method to Prepare Monodisperse Fe₃O₄ Microspheres with Controllable Sizes and Morphologies[J].Acta Phys. -Chim. Sin., 2017, 33(11): 2310-2316.

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A Time-Saving Method to Prepare Monodisperse Fe₃O₄ Microspheres with Controllable Sizes and Morphologies

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A Time-Saving Method to Prepare Monodisperse Fe₃O₄ Microspheres with Controllable Sizes and Morphologies