铁基多相助催化剂光电化学水氧化研究进展

doi:10.3866/PKU.WHXB202009022

Abstract

Abstract:

The use of fossil fuels has caused serious environmental problems such as air pollution and the greenhouse effect. Moreover, because fossil fuels are a non-renewable energy source, they cannot meet the continuously increasing demand for energy. Therefore, the development of clean and renewable energy sources is necessitated. Hydrogen energy is a clean, non-polluting renewable energy source that can ease the energy pressure of the whole society. The sunlight received by the Earth is 1.7× 10¹⁴ J in 1 s, which far exceeds the total energy consumption of humans in one year. Therefore, conversion of solar energy to valuable hydrogen energy is of significance for reducing the dependence on fossil fuels. Since Fujishima and Honda first reported on TiO₂ in 1972, it has been discovered that semiconductors can generate clean, pollution-free hydrogen through water splitting driven by electricity or light. Hydrogen generated through this approach can not only replace fossil fuels but also provide environmentally friendly renewable hydrogen energy, which has attracted considerable attention. Photoelectrochemical (PEC) water splitting can use solar energy to produce clean, sustainable hydrogen energy. Because the oxygen evolution reaction (OER) over a photoanode is sluggish, the overall energy conversion efficiency is considerably low, limiting the practical application of PEC water splitting. A cocatalyst is, thus, necessary to improve PEC water splitting performance. So far, the synthesis of first-row transition-metal-based (e.g., Fe, Co, Ni, and Mn) cocatalysts has been intensively studied. Iron is earth-abundant and less toxic than other transition metals, making it a good cocatalyst. In addition, iron-based compounds exhibit the properties of a semiconductor/metal and have unique electronic structures, which can improve electrical conductivity and water adsorption. Various iron-based catalysts with high activity have been designed to improve the efficiency of PEC water oxidation. This article briefly summarizes the research progress related to the structure, synthesis, and application of iron oxyhydroxides, iron-based layered double hydroxides, and iron-based perovskites and discusses the evaluation of the performance of these cocatalysts toward photoelectrochemical water oxidation.

Key words: Photoelectrochemical water splitting, Oxygen evolution reaction, Ferric hydroxide, Iron-based layered double hydroxide, Iron-based perovskites

Yan Li, Xingsheng Hu, Jingwei Huang, Lei Wang, Houde She, Qizhao Wang. Development of Iron-Based Heterogeneous Cocatalysts for Photoelectrochemical Water Oxidation[J]. Acta Phys. -Chim. Sin. 2021, 37(8), 2009022. doi: 10.3866/PKU.WHXB202009022

Figures/Tables 7

Photoanode	Photocurrent density change	The onset potential change	Illumination conditions	Ref.
WO₃@a-Fe₂O₃/FeOOH	0.3 to 1.12 mA·cm^-2 at 1.23 V vs. RHE	0.9 V to 0.78 V	AM 1.5G, 100 mW·cm^-2	14
V₂O₅/rGO/BiVO₄/FeOOH/NiOOH	0.25 to 3.06 mA·cm^-2 at 1.5 V vs. Ag/AgCl	0.5 V to 0.2 V	AM 1.5G, 100 mW·cm^-2	64
Fe₂O₃/FeOOH NFs on Au/Fe	1.45 to 3.1 mA·cm^-2 at 1.5 V vs. RHE	1 V to 0.7 V	AM 1.5G, 100 mW·cm^-2	65
FeOOH QDs/ZnO	0.21 to 0.44 mA·cm^-2 at 1.23 V vs. RHE	0.7 V to 0.4 V	AM 1.5G, 100 mW·cm^-2	69
h-FeOOH/Fe₂O₃	0.85 to 1.31 mA·cm^-2 at 1.23 V vs. RHE	0.92 V to 0.83 V	AM 1.5G, 100 mW·cm^-2	70
3C-SiC/FeOOH	0.52 to 0.73 mA·cm^-2 at 1.23 V vs. RHE	0.4 V to 0.2 V	AM 1.5G, 100 mW·cm^-2	71
β-FeOOH/BiVO₄	0.62 to 4.3 mA·cm^-2 at 1.23 V vs. RHE	0.8 V to 0.6 V	AM 1.5G, 100 mW·cm^-2	72
FeOOH/BiVO₄	1.1 to 2.3 mA·cm^-2 at 1.23 V vs. RHE	0.45 V to 0.3 V	AM 1.5G, 100 mW·cm^-2	73
rGO-α-Fe₂O₃/β-FeOOH	0.26 to 0.62 mA·cm^-2 at 1.23 V vs. RHE	0.88 V to 0.75 V	AM 1.5G, 100 mW·cm^-2	75
BiVO₄@Ni:FeOOH	0.25 to 2.86 mA·cm^-2 at 1.23 V vs. RHE	0.6 V to 0.4 V	AM 1.5G, 100 mW·cm^-2	76
FeOOH/H:BiVO₄	0.42 to 1.66 mA·cm^-2 at 1.23 V vs. RHE	0.95 V to 0.23 V	150 W Xe lamp, 100 mW·cm^-2	77
CuWO₄/CdS/FeOOH	0.58 to 2.05 mA·cm^-2 at 1.23 V vs. RHE	0.35 V to 0.25 V	AM 1.5G, 100 mW·cm^-2	78
Fe₂O₃/NiFeOOH	0.09 to 0.67 mA·cm^-2 at 1.23 V vs. RHE	1 V to 0.8 V	AM 1.5G, 100 mW·cm^-2	79
Ti-Fe₂O₃/FeOOH	nearly zero to mA·cm^-2 at 1.5 V vs. RHE	1 V to 0.92 V	AM 1.5G, 100 mW·cm^-2	80
ZnO/TiO₂/FeOOH	0.23 to 1.59 mA·cm^-2 at 1.8 V vs. RHE	0.41 V to 0.14 V	AM 1.5G, 100 mW·cm^-2	81
Fe₂O₃/FeOOH	0.83 to 0.91 mA·cm^-2 at 1.23 V vs. RHE	0.72 V to 0.63 V	AM 1.5G, 100 mW·cm^-2	82
WO₃/FeOOH	0.65 to 1.3 mA·cm^-2 at 1.23 V vs. RHE	0.7 V to 0.6 V	AM 1.5G, 100 mW·cm^-2	83
Co-FeOOH	0.69 to 4.71 mA·cm^-2 at 1.0 V vs. RHE	1.5 V to 1.23 V	AM 1.5G, 100 mW·cm^-2	84
Ni-FeOOH	0.69 to 2.55 mA·cm^-2 at 1.0 V vs. RHE	1.5 V to 1.23 V	AM 1.5G, 100 mW·cm^-2	84
WO₃/porous-BiVO₄/FeOOH	1.01 to 4.4 mA·cm^-2 at 1.23 V vs. RHE	0.3 V to 0.2 V	AM 1.5G, 100 mW·cm^-2	85
FeOOH/Fe₂O₃	1.55 to 2.4 mA·cm^-2 at 1.23 V vs. RHE	0.661 V to 0.582 V	AM 1.5G, 100 mW·cm^-2	86
FeOOH/rGO/BiVO₄	0.99 to 3.25 mA·cm^-2 at 1.23 V vs. RHE	0.35 V to 0.3 V	AM 1.5G, 100 mW·cm^-2	87
FeOOH/Fe₂O₃	0.612 to 1.21 mA·cm^-2 at 1.23 V vs. RHE	0.77 V to 0.65 V	AM 1.5G, 100 mW·cm^-2	88

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Photoanode	Photocurrent density change	The onset potential change	Illumination conditions	Ref.
BiVO₄/NiFe-LDH	0.5 to 1.58 mA·cm^-2 at 1.23 V vs. RHE	0.75 V to 0.32 V	AM 1.5G, 100 mW·cm^-2	97
NiFe-LDH/rGO/Fe₂O₃	0.45 to 0.95 mA·cm^-2 at 1.23 V vs. RHE	1.0 V to 0.85 V	AM 1.5G, 100 mW·cm^-2	101
TiO₂/BiVO₄/NiFe-LDH	6.9 to 17.6 μA·cm^-2 at 0.1 V vs. Ag/AgCl	0.74 V to 0.72 V	AM 1.5G, 100 mW·cm^-2	102
NiFe-LDH/BiVO₄	0.79 mA to 1.93 mA·cm^-2 at 1.23 V vs. RHE	0.7 V to 0.6 V	AM 1.5G, 100 mW·cm^-2	104
BiVO₄/Ni_0.5Fe_0.5-LDH	0.3 to 1.21 mA·cm^-2 at 1.23 V vs. RHE	0.47 V to 0.15 V	AM 1.5G, 100 mW·cm^-2	105
BiVO₄/Co_0.5Fe_0.5-LDH	0.3 to 1.05 mA·cm^-2 at 1.23 V vs. RHE	0.47 V to 0.18 V	AM 1.5G, 100 mW·cm^-2	105
WO₃/Fe₂O₃/NiFe-LDH	1.6 to 3.0 mA·cm^-2 at 1.8 V vs. RHE	0.2 V to 0.1 V	AM 1.5G, 100 mW·cm^-2	106
BiVO₄/rGO/NiFe-LDH	1.14 to 3.26 mA·cm^-2 at 1.23 V vs. RHE	similar onset potential	AM 1.5G, 100 mW·cm^-2	107
TiO₂/NiFe-LDH	0.92 to 1.18 mA·cm^-2 at 1.245 V vs. RHE	-0.2 V to -0.3 V	AM 1.5G, 100 mW·cm^-2	108
Ti-TiO_2-x@CoFe-LDH	0.65 to 0.78 mA·cm^-2 at 1.23 V vs. RHE	0.23 V to 0.18 V	AM 1.5G, 100 mW·cm^-2	109
CoFe-LDH/TNWs	0.33 to 3.0 mA·cm^-2 at 1.23 V vs. RHE	0.33 V to 0.22 V	AM 1.5G, 100 mW·cm^-2	110
CoFe-LDH@g-C₃N₄	0.061 to 0.196 mA·cm^-2 at 1.23 V vs. RHE	0.38 V to 0.346 V	AM 1.5G, 100 mW·cm^-2	111
NiFe-LDH/TiO₂	0.23 to 0.41 mA·cm^-2 at 1.23 V vs. RHE	0.36 V to 0.29 V	AM 1.5G, 100 mW·cm^-2	112
a-Fe₂O₃/NiFe-LDH	47 to 141 μA·cm^-2 at 1.23 V vs. RHE	0.5 V to 0.4 V	AM 1.5G, 100 mW·cm^-2	113
Mn:Fe₂O₃/NiFe-LDH	0.5 to 1.8 mA·cm^-2 at 1.23 V vs. RHE	0.7 V to 0.6 V	AM 1.5G, 100 mW·cm^-2	114

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Development of Iron-Based Heterogeneous Cocatalysts for Photoelectrochemical Water Oxidation

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