Acta Phys. -Chim. Sin. ›› 2025, Vol. 41 ›› Issue (6): 100055.doi: 10.1016/j.actphy.2025.100055
• ARTICLE • Previous Articles Next Articles
Insights into the greatly improved catalytic performance of N-doped BiOBr for CO2 photoreduction
Xianghai Song1,5, Xiaoying Liu1, Zhixiang Ren1, Xiang Liu2, Mei Wang3,*(
), Yuanfeng Wu4, Weiqiang Zhou1, Zhi Zhu1, Pengwei Huo1,*()
- 1 Institute of Green Chemistry and Chemical Technology, School of Chemistry and Chemical Engineering, Jiangsu University, Zhenjiang 212013, Jiangsu Province, China
2 Jiangsu Higher Vocational College Engineering Research Center of Green Energy and Low Carbon Materials, Zhenjiang College, Zhenjiang 212028, Jiangsu Province, China
3 School of Agricultural Engineering, Jiangsu University, Zhenjiang 212013, Jiangsu Province, China
4 School of Chemistry and Chemical Engineering, Henan Polytechnic University, Jiaozuo 454003, Henan Province, China
5 International Innovation Center for Forest Chemicals and Materials, Nanjing Forestry University, Nanjing 210037, Jiangsu Province, China
-
Received:2024-11-26Revised:2025-01-23Accepted:2025-01-23Published:2025-04-19 -
Contact:Email: 1000004927@ujs.edu.cn (Mei Wang)huopw@ujs.edu.cn (Pengwei Huo) -
Supported by:the National Natural Science Foundation of China(22108102); the National Natural Science Foundation of China(22078131); the Fundamental Research Funds for the Universities of Henan Province(NSFRF240609); the GHfund B(202302026857); the Science and Technology Planning Social Development Project of Zhenjiang City(SH2023102); the International Innovation Center for Forest Chemicals and Materials of Nanjing Forestry
Cite this article
Xianghai Song, Xiaoying Liu, Zhixiang Ren, Xiang Liu, Mei Wang, Yuanfeng Wu, Weiqiang Zhou, Zhi Zhu, Pengwei Huo. Insights into the greatly improved catalytic performance of N-doped BiOBr for CO2 photoreduction[J]. Acta Phys. -Chim. Sin. 2025, 41(6), 100055. doi: 10.1016/j.actphy.2025.100055
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Fig 1
(a) XRD patterns of the prepared samples, (b) electron spin resonance, (c) N2 adsorption-desorption isotherms and pore size distribution, (d) CO 2 adsorption isotherms of the BiOBr and 2N-BiOBr."
Fig 1
Table 1
Summarized N2 physisorption data for BiOBr and 2N-BiOBr."
| Sample | Specific surface area (m2·g−1) | Pore volume (cm3·g−1) | Average pore diameter (nm) |
| BiOBr | 2.95 | 0.01 | 10.01 |
| 2N-BiOBr | 6.45 | 0.04 | 30.38 |
Table 1
Fig 2
SEM patterns of (a, b) BiOBr, (c, d) 2N-BiOBr, and (e-g) elemental mapping images of 2N-BiOBr showing the elemental distribution of N, Bi and O elements."
Fig 2
Fig 3
XPS spectra of BiOBr and 2N-BiOBr: (a) Bi 4f, (b) O 1s, (c) Br 3d and (d) N 1s."
Fig 3
Fig 4
(a) UV-Vis DRS, (b) Tauc plots, (c) VB-XPS spectra and (d) band structure of the best photocatalyst and possible photocatalytic CO2 reduction mechanism of BiOBr and 2N-BiOBr."
Fig 4
Fig 5
(a) The transient photocurrent responses of BiOBr, 1N-BiOBr, 2N-BiOBr, 3N-BiOBr and 5N-BiOBr, (b) EIS spectrum of BiOBr, 1N-BiOBr, 2N-BiOBr and 3N-BiOBr, (c) linear sweep voltammogram (LSV) curves in CO2 atmosphere, (d) PL spectra, (e) Time-resolved PL spectra and (f) capacitance currents of BiOBr and 2N-BiOBr."
Fig 5
Table 2
PL decay lifetimes parameters."
| Catalysts | τ1 (ns) | τ2 (ns) | B1 | B2 | τav (ns) a |
| BiOBr | 16.36 | 126.15 | 3164.14 | 256.72 | 58.61 |
| 2N-BiOBr | 18.84 | 169.59 | 2955.06 | 183.35 | 72.86 |
Table 2
Fig 6
(a) Photocatalytic yield of BiOBr, 1N-BiOBr, 2N-BiOBr, 2NH4Cl-BiOBr 3N-BiOBr, 5N-BiOBr, 6N-BiOBr, and 2NH4OH-BiOBr, (b) photocatalytic yield of 2N-BiOBr under different conditions, (c) cycling performances of 2N-BiOBr and (d) The XRD patterns of the 2N-BiOBr before and after reaction."
Fig 6
Table 3
Data of the CO2 photoreduction performance of different photocatalysts"
| catalyst | Sacrificial agent | CO evolution (μmol·g−1·h−1) | Ref. |
| 2N-BiOBr | − | 18.28 | This work |
| Vo-R Bi24O31Br10 | − | 14.80 | [ |
| BiOBr-4 | − | 4.45 | [ |
| NH2-MIL- 53(Fe) | TEOA | 17.52 | [ |
| Ce/ZnFe2O4 | − | 1.7 | [ |
| SnFe2O4/α- Fe2O3 | − | 2.87 | [ |
| ZnIN2S4/BiVO4 | − | 4.75 | [ |
| P/Bi-BOB-0.25 | − | 3.1 | [ |
| Co-BiOBr-0.5 | − | 11.71 | [ |
| BSB-16 | − | 7.4 | [ |
| BiOBr0.6Cl0.4 | − | 15.86 | [ |
Table 3
Fig 7
In situ FTIR adsorption curve of (a) BiOBr, (b) 2N-BiOBr at a flow rate of 10 mL min−1 CO2/H2O (DRIFTS spectra), dark conditions, 0-30 min, Peak area integration of adsorbed (c) CO2 and (d) H2O at different time on BiOBr and 2N-BiOBr."
Fig 7
Fig 8
(a) In situ FTIR spectra of BiOBr, 2N-BiOBr during CO2 reduction under 420 nm light irradiation for 15 min (3W, LED), (b) amplified in situ FTIR spectra of BiOBr."
Fig 8
Fig 9
(a) Structure schematic of 2N-BiOBr, adsorption model and adsorption energy of CO2 on (b) BiOBr, and (c) 2N-BiOBr and (d) a potential reaction pathway for the photocatalytic reduction of CO2."
Fig 9
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