Acta Phys. -Chim. Sin. ›› 2026, Vol. 42 ›› Issue (7): 100225.doi: 10.1016/j.actphy.2025.100225
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Metal-Organic Frameworks (2014–2024): A decade pursuit for top performance
Ri Peng1, Yuxin Xie1, Shuai Yuan2, Ruwei Shen1, Dunru Zhu1,2,*(
)
- 1 State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, Nanjing Tech University, Nanjing 211816, Jiangsu Province, China
2 State Key Laboratory of Coordination Chemistry, Nanjing University, Nanjing 210023, Jiangsu Province, China
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Received:2025-09-22Revised:2025-11-23Accepted:2025-11-26Published:2026-05-22 -
Contact:Email: zhudr@njtech.edu.cn (Dunru Zhu)
Cite this article
Ri Peng, Yuxin Xie, Shuai Yuan, Ruwei Shen, Dunru Zhu. Metal-Organic Frameworks (2014–2024): A decade pursuit for top performance[J]. Acta Phys. -Chim. Sin. 2026, 42(7), 100225. doi: 10.1016/j.actphy.2025.100225
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Fig 1
Two "milestone" complexes: (a) [Co(HBTC)(Py)2]·2/3Py and (b) MOF-5 in the development of MOFs [1, 2]. Adapted with permission from Ref. [1] and [2], Copyright 1995 and 1999 Springer Nature publisher."
Fig 2
The number of MOF publications each year from 2014 to 2024. Web of Science data by searching the topic of "metal-organic framework" on August 31, 2025."
Table 1
MOFs with the best values for the indicated properties."
| Property or application | MOF | Achieved value | Refs. |
| Highest reported value | |||
| BET surface area a | NU-1501-Al b | 7310 m2 g−1 | [ |
| Cage size | MOF-939 | 11.4 nm | [ |
| Unit cell volume | NU-1301 | 5201294 Å3 | [ |
| Unit cell length | SC-MOF-6 c | 266.21 Å | [ |
| Thermal stability | MAF-stu-1 d | 680 ℃ | [ |
| Chemical stability | Cr-btec-tpt e | pH: −1.1~15 | [ |
| Volumetric H2 uptake (298 K/100 bar) | [Ni2(4,6-m-DOT)] | 11.9 g L−1 | [ |
| Usable H2 capacity (298 K/100 bar) | [Ni2(4,6-m-DOT)] | 11.0 g L−1 | [ |
| Gravimetric H2 uptake (296 K/100 bar) | NU-1501-Al | 2.9 wt% | [ |
| Usable CH4 capacity (298 K/65 bar) | [Co(bdp)] f | 197 cm3 cm−3 | [ |
| Gravimetric CH4 uptake (296 K/100 bar) | NU-1501-Al | 0.54 g g−1 | [ |
| Gravimetric NH3 uptake (298 K/1 bar) | LiCl@MIL-53-(OH)2 g | 0.58 g g−1 | [ |
| Volumetric NH3 uptake (298 K/1 bar) | LiCl@MIL-53-(OH)2 | 0.80 g cm−3 | [ |
| Gravimetric CO2 uptake (273 K/1 bar) | CPM-231 h | 0.46 g g−1 | [ |
| Proton conductivity (−40 ℃) | H2SO4@MIL-101-SO3H | 9.2 × 10−3 S cm−1 | [ |
| Proton conductivity (90 ℃/90% RH) i | LiCl@UiO-66-F2-(SO3H)2 j | 2.86 S cm−1 | [ |
| Gravimetric water uptake (RT/70% RH) k | Cr-soc-MOF-1 | 1.95 g g−1 | [ |
| Lowest reported value | |||
| Density | NU-1301 | 0.124 g cm−3 | [ |
Fig 3
(a) Synthetic strategy of NU-1501-Al. (b) Some porous MOFs with both ultrahigh volumetric and gravimetric BET areas [12]. Adapted with permission from Ref. [12], Copyright 2020 The American Association for the Advancement of Science publisher."
Fig 4
(a) Definition of expansion efficiency. (b) Construction principle of 3D MOF-939 with the largest cage [13]. Adapted with permission from Ref. [13], Copyright 2023 American Chemical Society publisher."
Fig 5
(a) Single cuboctahedron consisting of 8 [UO2(CO2)3]− SBUs and 12 L3− linkers. (b) A triangular face links two cuboctahedron cages. (c) The pentagonal prism consisting of 5 cuboctahedra and the hexagonal prism consisting of 6 cuboctahedra. (d) The large cages along different directions [14]. Adapted with permission from Ref. [14], Copyright 2017 The American Association for the Advancement of Science publisher."
Fig 6
(a) Coordination environment of Zn2+. (b) Thermal stability of [Zn(imPim)]. (c) Chemical stability of [Zn(imPim)] [16]. Adapted with permission from Ref. [16], Copyright 2019 John Wiley and Sons publisher."
Fig 7
Construction strategy and chemical stability of (a) PCN-222(Fe) and (b) PCN-601 [31, 32]. Adapted with permission from Ref. [31], Copyright 2012 John Wiley and Sons publisher. Adapted with permission from Ref. [32], Copyright 2016 American Chemical Society publisher."
Fig 8
(a) A series of ultrastable pacs-MOFs built by a three-module synthesis strategy. (b) Comparison of ultrastable MOFs based on stable pH range. (c) Chemical stability of Cr-btec-tpt determined from PXRD. Chemical stability of (d) CPM-243(F) and (e) Cr-btec-tpt based on N2 isotherms at 77 K [17, 33]. Adapted with permission from Ref. [33], Copyright 2021 American Chemical Society publisher. Adapted with permission from Ref. [17], Copyright 2024 John Wiley and Sons publisher."
Fig 9
(a) Comparison of total H2 uptake between pure compressed H2 and [Ni2(4,6-m-DOT)] at 100 bar. (b) A pore of [Co2(4,6-m-DOT)] with seven different D2 binding sites [18]. Adapted with permission from Ref. [18], Copyright 2018 American Chemical Society publisher."
Fig 10
(a) Some top-performing MOFs with both gravimetric and volumetric H2 working capacities. (b) Three main cages in NPF-200 [37]. Adapted with permission from Ref. [37], Copyright 2020 John Wiley and Sons publisher."
Fig 11
(a) Composition of MOF-519. (b) The volumetric CH4 storage in MOF-519. (c) Some top performing MOFs with CH4 working capacity [42]. Adapted with permission from Ref. [42], Copyright 2014 American Chemical Society publisher."
Fig 12
(a) A non-porous structure (0 bar) and a porous network (30 bar) of [Co(bdp)]. (b) Total CH4 adsorption isotherms of [Co(bdp)] [19]. Adapted with permission from Ref. [19], Copyright 2015 Springer Nature publisher."
Fig 13
(a) A schematic of preparing LiCl@MIL-53-(OH)2 and the selectively capturing ammonia. (b) NH3 uptake isotherms under 1 bar and RT. (c) 15 cycles of adsorption-desorption [20]. Adapted with permission from Ref. [20], Copyright 2022 John Wiley and Sons publisher."
Fig 14
(a) The schematic of novel In-MOF for caption of NH3. (b) NH3 adsorption isotherms of In-MOF under 1 bar and 0 ℃. (c) 10 cycles of NH3 adsorption-desorption [43]. Adapted with permission from Ref. [43], Copyright 2024 Royal Society of Chemistry publisher."
Fig 15
(a) Construction of CPM-231. (b) CO2 sorption of CPM-231 at 1 bar and 0 ℃ [21]. Adapted with permission from Ref. [21], Copyright 2016 Springer Nature publisher."
Fig 16
(a) The residual H2O shown as pink within micropore of Cu-F-pymo. (b) The CO2 and C2H2 sorption isotherms of Cu-F-pymo-a at 1 bar and RT. (c) Selectivity of CO2/C2H2 and uptake ratio in some MOF materials [51]. Adapted with permission from Ref. [51], Copyright 2021 John Wiley and Sons publisher."
Fig 17
(a) Cage A [Mn86] consisting of 6 [Mn8O12], 8 [Mn4O4] clusters and 6 discrete Mn2+ cations. (b) The gas uptake isotherm at RT and 1 bar [52]. Adapted with permission from Ref. [52], Copyright 2023 John Wiley and Sons publisher."
Fig 18
(a) A pore in ZnH-MFU-4l. (b) Varying-temperature CO2 adsorption (●) and desorption (○) isotherms. (c) The adsorption-desorption cycles of 508 [56]. Adapted with permission from Ref. [56], Copyright 2024 The American Association for the Advancement of Science publisher."
Fig 19
(a) The fsc framework of ZJU-300. (b) The C2H2 binding sites in the cavity of ZJU-300a. (c) Plot of C2H2/C2H4 selectivity versus 0.01-bar acetylene uptake for the top-performing materials [61]. Adapted with permission from Ref. [61], Copyright 2023 The American Association for the Advancement of Science publisher."
Fig 20
(a) 3D net in MIL-101-SO3H (SO3H group as yellow ball; Cr3+ cations as green polyhedra) and schematic of preparing H2SO4@MIL-101-SO3H. (b) Nyquist plot of H2SO4@MIL-101-SO3H (3 mol L−1) and the superprotonic conductivity [22]. Adapted with permission from Ref. [22], Copyright 2017 American Chemical Society publisher."
Fig 21
(a) Preparative route for LiCl@UiO-66-F2(SO3H)2. (b) CLMPC mechanism. (c) Nyquist plots of LiCl@UiO-66-F2(SO3H)2 under variable-temperature and 90% RH. (d) Some top performing materials with proton conductivities at 90% RH [23]. Adapted with permission from Ref. [23], Copyright 2023 American Chemical Society publisher."
Fig 22
Schematic of the MOF-based monocyclic AWH device containing a water adsorptive unit in a case [73]. Adapted with permission from Ref. [73], Copyright 2018 The American Association for the Advancement of Science publisher."
Fig 23
(a) Schematic for Cr-soc-MOF-1 capturing H2O double its weight. (b) H2O adsorption (●)/desorption (○) isotherm for activated Cr-soc-MOF-1 under RT. (c) Plot of H2O absorption vs. pore volume for some top-performing materials [24]. Adapted with permission from Ref. [24], Copyright 2018 Elsevier publisher."
Fig 24
MOF-based biosensing methods for pathogen detection [83]. Adapted with permission from Ref. [83], Copyright 2023 Elsevier publisher."
Fig 25
Schematic of 2D porphyrin-based heterobimetallic MOF, [(ZnTCPP)Co2(MeIm)], and its ECL biosensing to detect SARS-CoV-2 RdRp gene [89]. Adapted with permission from Ref. [89], Copyright 2022 John Wiley and Sons publisher."
Fig 26
Schematic of MOFs used for UES for the substantial nuclear energy [102]. Adapted with permission from Ref. [102], Copyright 2023 John Wiley and Sons publisher."
Fig 27
(a) Comparison of the U adsorption capacity of ZIF-67 with other MOFs sorbents. (b) Proposed adsorption mechanism of UO22+ by the ZIF-67 microcrystals [97]. Adapted with permission from Ref. [97], Copyright 2018 Elsevier publisher."
Fig 28
(a) Schematic of selective capturing UO22+ from the other cations by i-MZIF-90(50). (b) The UO22+ uptake in seawater during 25 days. (c) Plot of UO22+ uptake capacity vs. time for some top-performing sorbents in natural seawater [98]. Adapted with permission from Ref. [98], Copyright 2022 Royal Society of Chemistry publisher."
Fig 29
Schematic for four kinds of mixed-component MOFs and their typical examples. (a) Multivariate MOFs (MTV-MOF-5). (b) Multicomponent MOFs (UMCM-1). (c) Mixed-metals MOFs (MM-MOF-74). (d) Mixed-ligands and metals MOFs (MLM-CPM-231) [125]. Adapted with permission from Ref. [125], Copyright 2022 Elsevier publisher."
Fig 30
The roles LLMs can take in a data-driven selection process for synthesis of MOFs [159]. Adapted with permission from Ref. [159], Copyright 2025 Springer Nature publisher."
Fig 31
(a) Inverse reticular design strategy for non-MOFs. (b) Structures of organic bases used as linkers. (c) Space-filling structures of three non-MOFs TAPT.Cl, TT.Br, TTBT.Cl [167]. Adapted with permission from Ref. [167], Copyright 2024 Springer Nature publisher."
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