Acta Phys. -Chim. Sin. ›› 2026, Vol. 42 ›› Issue (7): 100287.doi: 10.1016/j.actphy.2026.100287
• ARTICLE • Previous Articles Next Articles
Charge redistribution on Pd mediated by electronically asymmetric carbon for boosting ethanol oxidation
Xincan Zhou1,2, Xueyao Wang1,3, Xiaokang Chen1,4, Di Lan2, Yuting Gao5, Xiaoxia Wang1, Daohao Li1, Shuchao Zhang1,6,*(
), Lijie Zhang1,*(), Guanglei Wu1,*()
- 1 State Key Laboratory of Bio-fibers and Eco-textiles, College of Materials Science and Engineering, Qingdao University, Qingdao 266237, Shandong Province, China
2 School of Automotive Materials, Hubei University of Automotive Technology, Shiyan 442002, Hubei Province, China
3 School of Environmental Science and Engineering, Shandong University, Qingdao 266237, Shandong Province, China
4 Institute of Frontier Chemistry, School of Chemistry and Chemical Engineering, Shandong University, Qingdao 266237, Shandong Province, China
5 Shandong Institute of Scientific and Technical Information, Jinan 250101, Shandong Province, China
6 Department of Blood Transfusion, The Affiliated Hospital of Qingdao University, Qingdao University, Qingdao 266003, Shandong Province, China
-
Received:2025-12-19Revised:2026-03-12Accepted:2026-03-12Published:2026-05-22 -
Contact:Email: zhangshuchao@qdu.edu.cn (Shuchao Zhang)lijiezh@qdu.edu.cn (Lijie Zhang)wuguanglei@qdu.edu.cn/wuguanglei@mail.xjtu.edu.cn (Guanglei Wu)
Cite this article
Xincan Zhou, Xueyao Wang, Xiaokang Chen, Di Lan, Yuting Gao, Xiaoxia Wang, Daohao Li, Shuchao Zhang, Lijie Zhang, Guanglei Wu. Charge redistribution on Pd mediated by electronically asymmetric carbon for boosting ethanol oxidation[J]. Acta Phys. -Chim. Sin. 2026, 42(7), 100287. doi: 10.1016/j.actphy.2026.100287
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Fig 1
Pd electronic structure based on DFT calculation (a–c) The optimized structures and the charge density differences of Pd@C, Pd@NC and Pd@SNC, respectively. Gray, purple, royalblue, and yellow balls represent C, Pd, N, and S atoms, respectively. The yellow and green regions indicate charge accumulating and charge depleting, respectively. (d) The PDOS curves of the surface Pd atom in the Pd@C, Pd@NC, and Pd@SNC (the Fermi level is set at zero energy)."
Fig 1
Fig 2
Preparation of Pd@SNC Illustration for Pd@SNC synthesis."
Fig 2
Fig 3
Characterization of samples (a) SEM images of Pd@SNC, TEM images of (b) Pd@C, (c) Pd@NC and (d) Pd@SNC (the inset is the corresponding size distribution), (e) HRTEM image of Pd@SNC, (f) HRTEM image of individual nanoparticle, corresponding FFT shown in inset, (g) XRD spectra of the three samples, (h) Raman spectra of Pd@C, Pd@NC and Pd@SNC, (i) N2 adsorption-desorption isotherms, (j) Surface areas and pore sizes of Pd@C, Pd@NC and Pd@SNC and (k) TEM-EDS mapping of Pd@SNC."
Fig 3
Fig 4
Structural Characterization of samples The high-resolution XPS survey scan spectra (a) S 2p, (b) N 1s of Pd@SNC. (c) Pd 3d of Pd@SNC, Pd@NC and Pd@C. (d) XANES spectra at Pd L-edge of Pd@SNC, Pd@NC and Pd@C, (e, f) FT-EXAFS spectra and WT-EXAFS of Pd@SNC, Pd@NC and Pd@C."
Fig 4
Fig 5
The EOR activities of samples EOR performances of different electrocatalysts in N2-saturated 1 mol L−1 KOH + 1 mol L−1 ethanol solution. (a) CV curves, (b) specific and mass activities at peak potentials, (c) Mass activities and If/Ib ratios, (d) Tafel plots, (e) specific activities after different scan cycles, (f) CV curves of Pd@SNC at different cycles with a scanning rate of 50 mV s−1, (g) chronoamperometric (CA) tests at 0.8 V and (h) long-time durability, the arrows indicate when the electrolyte is refreshed."
Fig 5
Fig 6
Reaction mechanism (a) The adsorption of OH− on Pd surface, (b) Free-energy diagram and (c) The energy value of each reaction step for Pd@C, Pd@NC and Pd@SNC, (d) Schematic illustration of the mechanism for EOR on Pd@SNC."
Fig 6
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