WO3/In2S3 S型异质结中通过W-S键的界面电子转移增强光催化产H2O2

doi:10.1016/j.actphy.2026.100357

物理化学学报 >> 2026, Vol. 42 >> Issue (11): 100357.doi: 10.1016/j.actphy.2026.100357

WO₃/In₂S₃ S型异质结中通过W-S键的界面电子转移增强光催化产H₂O₂

朱文君¹, 施锦¹, 张勇¹, 闫盼盼², 李猛³, 别传彪²

1 湖北理工学院新材料与绿色化工学院, 矿区环境污染控制与修复湖北省重点实验室, 湖北黄石 435003;
2 中国地质大学太阳燃料实验室, 材料与化学学院, 湖北武汉 430078;
3 南宁师范大学广西天然高分子化学与物理重点实验室, 广西壮族自治区南宁 530001

收稿日期:2026-06-07 修回日期:2026-06-27 录用日期:2026-07-02 发布日期:2026-09-29
通讯作者: 李猛, 别传彪 E-mail:limeng_2016@126.com;biechuanbiao@cug.edu.cn
基金资助:
本研究得到了湖北理工学院人才引进计划(编号：24xjz12R)；湖北省教育厅研究项目(编号：Q20244508)；湖北省自然科学基金创新发展联合基金黄石重点项目(编号：2025AFD004)；国家自然科学基金(项目批准号：22378103和52272290)；湖北省自然科学基金(编号：2025AFB492)以及中国地质大学(武汉)人才岗位科研启动经费资助(项目编号：2025097)的资助。

Interfacial electron transfer in WO₃/In₂S₃ S-scheme heterojunctions via W-S bonds for enhanced photocatalytic H₂O₂ production

Wenjun Zhu¹, Jin Shi¹, Yong Zhang¹, Panpan Yan², Meng Li³, Chuanbiao Bie²

1 School of Advanced Materials and Green Chemical Engineering, Hubei Key Laboratory of Mine Environmental Pollution Control & Remediation, Hubei Polytechnic University, Huangshi 435003, Hubei Province, China;
2 Laboratory of Solar Fuel, Faculty of Materials Science and Chemistry, China University of Geosciences, Wuhan 430078, Hubei Province, China;
3 Guangxi Key Laboratory of Natural Polymer Chemistry and Physics, Nanning Normal University, Nanning 530001, Guangxi Zhuang Autonomous Region, China

Received:2026-06-07 Revised:2026-06-27 Accepted:2026-07-02 Published:2026-09-29
Contact: Meng Li, Chuanbiao Bie E-mail:limeng_2016@126.com;biechuanbiao@cug.edu.cn

1. 2026.100357-ACTPHY-D-26-00379-16p-2# Supporting Information.pdf(1518KB)

摘要/Abstract

摘要： 梯型(S型)异质结因其独特的电荷转移机制以及最大化光生电子和空穴的氧化还原能力而脱颖而出，已被广泛用于应对日益严峻的能源危机和环境挑战。本文通过界面W-S配位键在多孔WO₃纳米纤维上生长In₂S₃纳米片，开发了无贵金属的WO₃/In₂S₃ S型异质结。在WO₃/In₂S₃异质界面形成的W-S键构建了快速电荷传输通道，加速了载流子分离，并促进了光催化H₂O₂的生成。优化后的WO₃/In₂S₃复合材料(WI-25)实现了1349.2 μmol g^-1 h^-1的优异光催化H₂O₂产率。原位辐照X射线光电子能谱(ISI-XPS)、偏态密度(PDOS)计算、电子顺磁共振(EPR)和飞秒瞬态吸收光谱(fs-TAS)共同验证了由界面配位键介导的S型电荷转移路径。本研究为构建具有界面配位键的S型异质结以提高光催化性能提供了一种合理策略。

关键词: 光催化, S型异质结, 界面电荷转移, 过氧化氢, 三氧化钨

Abstract: Step-scheme (S-scheme) heterojunctions stand out owing to their unique charge transfer mechanism and the maximized redox capacities of photoexcited electrons and holes, and have been widely exploited to address the ever-growing energy crisis and environmental challenges. Herein, noble-metal-free WO₃/In₂S₃ S-scheme heterojunctions have been developed by growing In₂S₃ nanosheets on porous WO₃ nanofibers via interfacial W-S coordination bonds. The W-S bonds formed at the WO₃/In₂S₃ heterointerface construct rapid charge transport channels, accelerate carrier separation, and boost photocatalytic H₂O₂ evolution. The optimized WO₃/In₂S₃ composite (WI-25) delivers an outstanding photocatalytic H₂O₂ yield of 1349.2 μmol g^-1 h^-1. In situ irradiated X-ray photoelectron spectroscopy (ISI-XPS), partial density of states (PDOS) calculations, electron paramagnetic resonance (EPR), and femtosecond transient absorption spectroscopy (fs-TAS) collectively verify the S-scheme charge transfer pathway mediated by interfacial coordination bonds. This work offers a rational strategy for constructing S-scheme heterojunctions with interfacial coordination bonds to improve photocatalytic performance.

Key words: Photocatalysis, S-scheme heterojunction, Interfacial charge transfer, Hydrogen peroxide, Tungsten trioxide

朱文君, 施锦, 张勇, 闫盼盼, 李猛, 别传彪. WO₃/In₂S₃ S型异质结中通过W-S键的界面电子转移增强光催化产H₂O₂[J]. 物理化学学报, 2026, 42(11), 100357. doi: 10.1016/j.actphy.2026.100357

Wenjun Zhu, Jin Shi, Yong Zhang, Panpan Yan, Meng Li, Chuanbiao Bie. Interfacial electron transfer in WO₃/In₂S₃ S-scheme heterojunctions via W-S bonds for enhanced photocatalytic H₂O₂ production[J]. Acta Phys. -Chim. Sin. 2026, 42(11), 100357. doi: 10.1016/j.actphy.2026.100357

链接本文: https://www.whxb.pku.edu.cn/CN/10.1016/j.actphy.2026.100357

https://www.whxb.pku.edu.cn/CN/Y2026/V42/I11/100357

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WO₃/In₂S₃ S型异质结中通过W-S键的界面电子转移增强光催化产H₂O₂

Interfacial electron transfer in WO₃/In₂S₃ S-scheme heterojunctions via W-S bonds for enhanced photocatalytic H₂O₂ production

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