回收造纸污泥制备低成本Ni改性碳/硅复合材料用于高效微波吸收

doi:10.1016/j.actphy.2026.100417

物理化学学报 >> 2026, Vol. 42 >> Issue (11): 100417.doi: 10.1016/j.actphy.2026.100417

论文上一篇

回收造纸污泥制备低成本Ni改性碳/硅复合材料用于高效微波吸收

朱保顺¹, 王薪琰¹, 牟维鹏¹, 孙轩鹏¹, 王昱博¹, 卫泓妤¹, 石庞玉¹, 郝惠兰¹, 王大双⁴, 力国民², 王桂振³

1 山西科技学院材料科学与工程学院, 山西晋城 048011;
2 太原科技大学材料科学与工程学院, 山西太原 030024;
3 海南大学材料科学与工程学院精密仪器高等研究中心, 海南海口 570228;
4 湖北汽车工业学院汽车材料学院, 湖北十堰 442002

收稿日期:2026-06-09 修回日期:2026-08-22 录用日期:2026-08-31 发布日期:2026-09-29
通讯作者: 朱保顺, 力国民, 王桂振 E-mail:zhubaoshun@sxist.edu.cn;ligm@tyust.edu.cn;wangguizhen@hainanu.edu.cn
基金资助:
本工作得到了山西省自然科学基金(202303021222293、202303021222290)，国家自然科学基金(52572138)以及山西科技学院高层次人才科研启动基金(2023015)的资助。

Recycling paper mill sludge to prepare low-cost Ni-modified carbon/silica composite for efficient microwave absorption

Baoshun Zhu¹, Xinyan Wang¹, Weipeng Mu¹, Xuanpeng Sun¹, Yubo Wang¹, Hongyu Wei¹, Pangyu Shi¹, Huilan Hao¹, Dashuang Wang⁴, Guomin Li², Guizhen Wang³

1 School of Materials Science and Engineering, Shanxi Institute of Science and Technology, Jincheng 048011, Shanxi Province, China;
2 School of Materials Science and Engineering, Taiyuan University of Science and Technology, Taiyuan 030024, Shanxi Province, China;
3 Center for Advanced Studies in Precision Instruments School of Material Science and Engineering, Hainan University, Haikou 570228, Hainan Province, China;
4 School of Automotive Materials, Hubei University of Automotive Technology, Shiyan 442002, Hubei Province, China

Received:2026-06-09 Revised:2026-08-22 Accepted:2026-08-31 Published:2026-09-29
Contact: Baoshun Zhu, Guomin Li, Guizhen Wang E-mail:zhubaoshun@sxist.edu.cn;ligm@tyust.edu.cn;wangguizhen@hainanu.edu.cn

1. ACTPHY-D-26-00384-SI.pdf(470KB)

摘要/Abstract

摘要： 生物质衍生的磁介电协同复合材料因其来源广泛、成本低廉和结构独特而在微波吸收领域受到广泛关注。本研究通过脱矿-浸渍-烧结工艺，成功制备了造纸污泥(PMS)衍生的Ni改性C/SiO₂(Ni/C/SiO₂)复合材料。通过调节烧结温度，优化了Ni颗粒分布以及多孔碳骨架与内部灰分SiO₂的复合，增强了磁介电协同效应，实现了优异的阻抗匹配和电磁波衰减。特别是Ni/C/SiO₂复合材料在700 ℃热处理温度下(NCS-700)表现出优异的微波吸收性能，在匹配厚度为2.0 mm时，有效吸收带宽(EAB)达到5.6 GHz，最小反射损耗(RL_min)为-39.2 dB。这种优异的性能源于多重损耗机制的协同增强，包括偶极子/界面极化弛豫、导电损耗和磁损耗。这项工作不仅为造纸污泥回收利用开辟了新前景，也为设计宽频段微波吸收剂提供了一条简单且经济高效的途径。

关键词: 造纸污泥, 微波吸收, 阻抗匹配, 界面极化, 固废利用

Abstract: Biomass-derived magnetic-dielectric synergistic composites have drawn extensive attention for microwave absorption (MA) due to their wide sources, low-cost, and unique structures. In this work, Ni-modified carbon/silica (Ni/C/SiO₂) composites from paper mill sludge (PMS) were successfully synthesized using a combination of demineralization, impregnation, and sintering processes. By regulating the sintering temperature, the Ni particle distribution and the compositing of the porous carbon skeleton with SiO₂ present in internal ash were optimized, enhancing the magnetic-dielectric synergy and yielding superior impedance matching and electromagnetic wave attenuation. In particular, Ni/C/SiO₂ composite sintering at 700 ℃ (NCS-700) demonstrated excellent microwave absorption performance, achieving an effective absorption bandwidth (EAB) of 5.6 GHz and a minimum reflection loss (RL_min) of -39.2 dB at a matching thickness of 2.0 mm. This superior performance originates from the synergistic enhancement of multiple loss mechanisms, including dipole/interface polarization relaxation, conductive loss, and magnetic loss. This work not only opens up new prospects for PMS recycling but also provides a facile and cost-effective route to designing broadband microwave absorbers.

Key words: Paper mill sludge, Microwave absorption, Impedance matching, Interface polarization, Solid waste utilization

朱保顺, 王薪琰, 牟维鹏, 孙轩鹏, 王昱博, 卫泓妤, 石庞玉, 郝惠兰, 王大双, 力国民, 王桂振. 回收造纸污泥制备低成本Ni改性碳/硅复合材料用于高效微波吸收[J]. 物理化学学报, 2026, 42(11), 100417. doi: 10.1016/j.actphy.2026.100417

Baoshun Zhu, Xinyan Wang, Weipeng Mu, Xuanpeng Sun, Yubo Wang, Hongyu Wei, Pangyu Shi, Huilan Hao, Dashuang Wang, Guomin Li, Guizhen Wang. Recycling paper mill sludge to prepare low-cost Ni-modified carbon/silica composite for efficient microwave absorption[J]. Acta Phys. -Chim. Sin. 2026, 42(11), 100417. doi: 10.1016/j.actphy.2026.100417

链接本文: https://www.whxb.pku.edu.cn/CN/10.1016/j.actphy.2026.100417

https://www.whxb.pku.edu.cn/CN/Y2026/V42/I11/100417

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回收造纸污泥制备低成本Ni改性碳/硅复合材料用于高效微波吸收

Recycling paper mill sludge to prepare low-cost Ni-modified carbon/silica composite for efficient microwave absorption

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