面向海洋应用的多功能涂层：基于氟硅烷包覆CIP实现防腐、吸波与减阻一体化

doi:10.1016/j.actphy.2026.100292

物理化学学报 >> 2026, Vol. 42 >> Issue (11): 100292.doi: 10.1016/j.actphy.2026.100292

面向海洋应用的多功能涂层：基于氟硅烷包覆CIP实现防腐、吸波与减阻一体化

孙至民^1,2, 薛文宇^1,2, 杨爽爽^1,2, 张朝阳^1,2, 于波¹, 王行伟^1,2, 于强亮^1,2, 周峰¹, 刘维民^1,2

1 中国科学院兰州化学物理研究所固体润滑国家重点实验室, 甘肃兰州 730000;
2 山东烟台先进材料与绿色制造山东实验室, 山东烟台 264000

收稿日期:2026-02-11 修回日期:2026-03-22 录用日期:2026-03-24 发布日期:2026-09-29
通讯作者: 王行伟, 于强亮 E-mail:wangxingwei@licp.cas.cn;yql@licp.cas.cn
基金资助:
本研究得到国家自然科学基金(52305234, 52475226)；山东省自然科学基金(ZR2023QE329)；泰山学者计划(tsqn202312299)及甘肃省科技计划(23ZDGA011, 24JRRA043)的资助

Multifunctional coating for marine applications: simultaneously achieving corrosion resistance, microwave absorption, and drag reduction via fluorosilane-encapsulated CIPs

Zhimin Sun^1,2, Wenyu Xue^1,2, Shuangshuang Yang^1,2, Chaoyang Zhang^1,2, Bo Yu¹, Xingwei Wang^1,2, Qiangliang Yu^1,2, Feng Zhou¹, Weimin Liu^1,2

1 State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, Gansu Province, China;
2 Shandong Laboratory of Advanced Materials and Green Manufacturing at Yantai, Yantai 264000, Shandong Province, China

Received:2026-02-11 Revised:2026-03-22 Accepted:2026-03-24 Published:2026-09-29
Contact: Xingwei Wang, Qiangliang Yu E-mail:wangxingwei@licp.cas.cn;yql@licp.cas.cn

摘要/Abstract

摘要： 羰基铁粉(CIP)是一种典型的磁损耗型微波吸收材料。然而，其在严苛海洋环境(高湿度、高盐度)下易发生电化学腐蚀，导致性能退化，限制了长期应用。本研究通过溶胶-凝胶法将全氟癸基三甲氧基硅烷(PFOTES)包覆在CIP表面制备了核壳结构粒子(CIP@PFOTES)。随后将粒子掺入氟硅树脂(FSR-ZY220L)中，制得多功能CIP@PFOTES-ZY涂层。该涂层表现出超疏水性，水接触角达158°。在0.1-100 s^-1剪切速率范围内减阻率超过70%。中性盐雾环境中涂层展现出优异的长期耐腐蚀性能，电化学阻抗谱(EIS)表明在3.5 wt.% NaCl溶液中浸泡40 d后，低频阻抗模值(|Z|_0.01 Hz)仍保持在10⁷ Ω cm²以上。此外，1.3 mm厚度涂层获得7.52 GHz有效吸收带宽(EAB，RL ≤ -10 dB)，微波吸收性能较未改性样品显著提升。本研究为开发适用于严苛海洋环境的高性能、多功能防护涂层提供了一种有效的材料设计策略。

关键词: 羰基铁粉, 核壳结构, 耐腐蚀性, 微波吸收, 减阻, 超疏水性

Abstract: Carbonyl iron powder (CIP) is a typical magnetic loss-type microwave absorbing material. However, its susceptibility to electrochemical corrosion in harsh marine environments (characterized by high humidity and salinity) leads to performance degradation, limiting long-term applications. In this study, core-shell particles (CIP@PFOTES) were fabricated via a sol-gel method, encapsulating CIP with a perfluorodecyltrimethoxysilane (PFOTES) shell. These particles were then incorporated into a fluorosilicone resin (FSR-ZY220L) to produce a multifunctional CIP@PFOTES-ZY coating. The coating exhibited superhydrophobicity with a water contact angle of 158°. A drag reduction exceeding 70% was achieved at shear rates ranging from 0.1 to 100 s^-1. The coating demonstrated excellent long-term corrosion resistance in a neutral salt spray environment. Electrochemical impedance spectroscopy (EIS) indicated that after 40 d of immersion in a 3.5 wt.% NaCl solution, the low-frequency impedance modulus (|Z|_0.01 Hz) remained above 10⁷ Ω cm². Furthermore, with a thickness of 1.3 mm, the coating achieved an effective absorption bandwidth (EAB, RL ≤ -10 dB) of 7.52 GHz, demonstrating significantly superior microwave absorption performance compared to the unmodified counterpart. This study provides an effective material design strategy for developing high-performance, multifunctional protective coatings for marine applications.

Key words: Carbonyl iron powder, Core-shell structure, Corrosion resistance, Microwave absorption, Drag reduction, Superhydrophobicity

孙至民, 薛文宇, 杨爽爽, 张朝阳, 于波, 王行伟, 于强亮, 周峰, 刘维民. 面向海洋应用的多功能涂层：基于氟硅烷包覆CIP实现防腐、吸波与减阻一体化[J]. 物理化学学报, 2026, 42(11), 100292. doi: 10.1016/j.actphy.2026.100292

Zhimin Sun, Wenyu Xue, Shuangshuang Yang, Chaoyang Zhang, Bo Yu, Xingwei Wang, Qiangliang Yu, Feng Zhou, Weimin Liu. Multifunctional coating for marine applications: simultaneously achieving corrosion resistance, microwave absorption, and drag reduction via fluorosilane-encapsulated CIPs[J]. Acta Phys. -Chim. Sin. 2026, 42(11), 100292. doi: 10.1016/j.actphy.2026.100292

链接本文: https://www.whxb.pku.edu.cn/CN/10.1016/j.actphy.2026.100292

https://www.whxb.pku.edu.cn/CN/Y2026/V42/I11/100292

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面向海洋应用的多功能涂层：基于氟硅烷包覆CIP实现防腐、吸波与减阻一体化

Multifunctional coating for marine applications: simultaneously achieving corrosion resistance, microwave absorption, and drag reduction via fluorosilane-encapsulated CIPs

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